The kaolin was calcined in a muffle furnace at 800 °C for 10 h to remove hydroxyl Then the calcined kaolin and snail shell were ground at different ratios using a mortar The ground catalyst were added to different concentrations of KBr solution for 3 h 6 h with warm water then filtrated and placed in a drying oven at 110 °C for 12 h Finally the dried catalyst was calcined in a muffle
Get PriceBefore use kaolin was calcined at 650 °C for 2 h at a heating rate of 10 °C·min 1 to transform kaolin into MTK as well as to remove impurities The obtained MTK was used as a catalyst support in this study Nickel II nitrate hexahydrate Ni NO 3 2 ·6H 2 O purity >% Sigma Aldrich and cerium III nitrate hexahydrate Ce NO 3 3 ·6H 2 O purity >% Sigma Aldrich were
Get PriceThe BET SSA values of the raw and calcined kaolins are presented in Fig 10 The SSA of the kaolins were measured and found to be between 5500 8300 m 2 /kg and 4400 7400 m 2 /kg for raw and
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Get PriceThe dry beneficiated kaolin was calcined at 850°C in an electric furnace Nabertherm 30 1400°C for ‒34 The dried beneficiated kaolin was heated in a programmable furnace from room temperature to the desire temperature of 850°C at heating rate of 10°C/min The metakaolin obtained was cooled in a desiccators and then package for analysis Dealumination of metakaolin In a batch
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Get PriceThe residue product was then filtered repeatedly washed with distilled water to remove any unspent oxalic acid dried at 103 °C for 24 h Finally the acid treated hydrous kaolin was activated through thermal treatment in a muffled furnace at 700 °C for 3 h resulting in the formation of calcined kaolin see figure 1
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Get PriceThe chemical analysis for the raw kaolin revealed that the sample is very rich in ferric iron as depicted in Table 1 The high ferric iron content which imparts red colouration to the raw kaolin RRK renders this raw clay unfit for aesthetically related uses The raw beneficiated and calcined kaolin respectively have the following formulae
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